Quasi-static testing of new peel stopper design for sandwich structures Jakobsen J., Bozhevolnaya E., and Thomsen O.T. Department of Mechanical Engineering, Aalborg University Pontoppidanstraede 105, 9220 Aalborg, Denmark ABSTRACT In this paper a specially designed peel stopper will be presented [1]. The proposed peel stopper appears as a substructural component, which has to be embedded into the core of the sandwich element during its manufacturing. The peel stopper works by activating an internal mechanism that prevents the propagation of delamination beyond the peel stopper boundaries, and thus restricts damage to a limited area where the delamination/peeling was initiated. When delamination/peeling is locally confined to the allowable and a priori predicted damage areas, the structural integrity of the sandwich is preserved, and the development of global failure/collapse may efficiently be prevented. Three configurations of sandwich beams were manufactured and tested in 3 point bending under quasi-static load conditions. The first configuration had not been furnished with the peel stopper. The second configuration had an insert of the same material and of equal weight as the implemented peel stopper. The third configuration had the peel stoppers embedded. High-speed video recordings were performed during loading of the specimens up to failure, and post mortem inspections were subsequently conducted. The results of the tests showed that only the specimens with peel stoppers were able to arrest the crack propagation, thus ensuring that the material behind the peel stoppers remained intact and undamaged. Introduction A sandwich concept is a layered assembly made of two thin strong face sheets separated by and bonded to a compliant lightweight core. Such a lightweight structural element provides very high bending stiffness, very high strength and other useful properties like high thermal insulation, high internal damping, high corrosion resistance, low maintenance costs, etc. This makes sandwich structures to be well suited for applications in the aerospace, marine, automotive, sustainable energy industries as well as in civil engineering. However, sandwich elements are only functional with sub-structural internal components such as various inserts, edge stiffeners, core junctions, etc., which allow an assembling of the sandwich elements into complete structures and their subsequent practical usage. It is known that introducing the sub-structural components into sandwiches makes them vulnerable with respect to their structural integrity, because various stress concentrations might arise in the vicinity of the geometrical and material changes. The stress concentrations might lead to local and possibly global failures (damages) of the sandwich assembly. Impact, manufacturing flows or fatigue loading might also instigate damage and failure. General scenario for the sandwich failure is a presence of delamination between the face sheets and the core of the sandwich structure. Such delaminations may start without prior warning, propagate very fast and eventually lead to a complete failure and collapse of the sandwich structure. Initiation and propagation of cracks in sandwich structures are in focus of many reported and ongoing studies. Burman and Zenkert studied the fatigue behavior of initial damaged and undamaged sandwich structures loaded in four point bending [2,3]. They found that fatigue may start in the core and continue as a face/core delamination. Carlsson et al studied the influences from face/core debonds on the crack developments in sandwich panels under compressive loads [4-7]. They found that the debonded area propagated as a face/core delamination when the load reached the buckling/instability level of the sandwich panel. Furthermore Bozhevolnaya et al studied the influences of core junctions on the structural response [8-12]. They found that the fatigue life was very dependant on the shape of the particular internal core junctions, and face/core delamination was commonly observed as the failure mode. There is a known attempt by Grenestedt [13-14] to introduce a sub-structural element which stops the peeling of the face during delamination. The technique is shown to be effective but rather manufacture challenging. Therefore there is a need in developing a peel stopper, which would prevent/limit delamination in the sandwich structures and at the same time would be easy to implement from the technologic point of view. Peel Stopper Concept The basic design of the suggested peel stopper [1] is illustrated in Figure 1. The peel stopper is a sub-structural component embedded into the sandwich panel (like an insert or edge stiffener), and its main purpose is to arrest face-core interface crack propagation by rerouting the crack path into a closed/restricted area of the sandwich panel, thus preventing the spreading of debonding/delamination into the remaining parts of the sandwich structure. Figure 1 Proposed design of the peel stopper. The case shown displays a crack re-routing angle of 10 degrees. For the present study, the peel stoppers were manufactured from an elasto-plastic material, with elastic properties close to the sandwich core properties. Generally, it is recommended that the material of the peel stopper is chosen to be compliant and with large straining capability (i.e. ductile), and the elastic stiffness of the peel stopper is recommended to be of the same order as the elastic properties of the main sandwich core (or somewhat higher). Good adhesion properties with respect to both the core and the faces are required as well. The peel stoppers may be mounted into a sandwich panel (e.g. a sandwich beam, plate or shell), as shown in Figure 2, together with other sub-structural components like e.g. structural inserts. Essentially, there are no or only minor manufacturing difficulties associated with the introduction of the peel stoppers, since they are similar to insert types already widely used in sandwich structures. Figure 2 Suggested implementation of the proposed peel stoppers in a sandwich plate. The grid type pattern will confine damage to the grid mesh. Failure is often initiated by crack formation in the interior core parts of the sandwich structure due to fatigue load conditions, impact/shock (dynamic) loads or from manufacturing imperfections. Under such circumstances the core crack will often propagate towards a core-face interface, from where it usually proceeds as a delamination along the face-core interface. The principle idea of the new peel stopper concept is that propagation of delamination/debonding is prevented to spread beyond the boundaries of the proposed peel stoppers. This inhibition is due to a rerouting of the crack along the internal curve of the peel stopper (arrowed line) instead of propagation along the interface (dashed line), as shown schematically in Figure 3. This technique will confine the debonding/delamination to a limited area of a single grid of the peel stoppers (cf. Figure 2). Furthermore, the proposed peel stopper will allow the debonded sandwich face be kept attached to the sandwich component (contrary to the method described in [18,19]). This will retain some structural load carrying capability of the debonded structure after delamination/debonding, especially under in-plane tensile loading. Figure 3. The basic idea of the peel stopper is to force the crack to propagate along the stopper-core interface (internal curve arrowed line) and not along the face-core interface (dashed line). Test Specimens Verification and functionality tests of the proposed peel stopper design were performed by means of comparing three sandwich beam test configurations, denoted as (a), (b) and (c) in Figure 4. Figure 4 Three test configurations with Rohacell® foams and carbon fibre reinforced composite faces for the quasi-static validation of the peel stopper concept. These beams were manufactured with PMI Rohacell® cores. For each configuration (a, b, and c) two specimens were manufactured and tested quasi-statically in a three-point bending loading, as illustrated schematically in Fig. 4. The main purpose of the experiments was to induce a shear failure in the softer core of the sandwich beam, followed by crack propagation and crack-kinking towards the face-core interfaces and finally delamination along the interfaces. This allowed a detailed study of the influence of the presence of the peel stoppers on the propagation of completely developed delaminations. Each test specimen had a total length of 500mm and a beam span between the supports of 460mm. The beam configurations o o o (a), (b) and (c) were manufactured with a 1mm thick carbon fibre laminate face sheets. The lay up was (0 ,90 ,0 ) of both top and bottom faces. The core of these specimens consisted of two 25mm thick PMI foam core parts from Rohacell® with different densities (51WF and 200WF). The stiffer core, 200WF, was located at the edges of the beams, and an araldite diaphragm was placed in the beam centre to avoid indentation failure due to the external loading. In beam configurations (b) and (c), polyurethane inserts were embedded between the two cores as shown in Fig. 4. A conventional butt insert was used in configuration (b), and the proposed peel stopper was used in configuration (c). The material data are specified in Table 2. Table 1 Mechanical properties of the tested beams. Materials Test configurations (a), (b), (c) T700 UD/SE 84LV[23] – face Rohacell® 200WF[24] – edge core Rohacell® 51WF[24] – main core Test configurations (b) and (c) PERMAlock 40496 (PU)[25] – peel stopper All Test Configurations Araldite 2011 [27] – adhesive Araldite B30[26] – diaphragm E-Modulus [MPa] Tensile Strength [MPa] Compress. Strength [MPa] Elongation at failure [%] 129,200 350 75 2844 6.8 1.6 1187 9.0 0.8 3.5 3.0 100 10 - 25 3700 Shear lap strength 26MPa 60 100 5-6 Configurations (b) and (c) were designed to have equal mass and identical material composition. Configuration (a), which represents a realistic design configuration, was considered as a reference to evaluate the two other configurations against. Every test configuration shown in Figure 4 was manufactured by assembling and bonding the core prior to prepreg/face lamination using a vacuum bagging technique. The sandwich panel was cured for six hours at 100ºC, and afterwards postcured for 48 hours at room temperature. Finally, the sandwich panel was cut into separate beams with a final width of 58mm. All the tested configurations (a)-(c) were geometrically similar, and the only difference was the choice of material composition. The mechanical properties of the sandwich beams constituents are given in Table 1. Test Results The three-point bending scheme was chosen, as it provided a controlled shear cracking of the core in the bulk of the weaker foams. The shear cracks propagated towards the face sheets, where crack kinking occurred followed by crack propagation in a delamination mode along the face-core interfaces. An experimental set-up was designed and manufactured on the basis of a 100kN servo hydraulic Schenk Hydropuls® testing machine. The testing machine has four test regions, where the lowest region was used for this particular test setup. The upper load limit in this test region is 12.5kN, which gave a discrepancy between the input and output load signal of less than 3%. A load controlled mode was used during loading, which was performed with a load rate of 0.02kN/sec. The central deflection of all specimens was recorded via the displacement of the cross head. High-speed video recording of specimen failure was enabled with a frame rate of 6000 frames/sec. The observed flexural load vs. central deflection responses of configurations (a)–(c) shown in Figure 5 were very similar as expected. This is an indication that the overall structural stiffness of the sandwich beam was not affected by the introduction of the peel stoppers. Figure 5 Applied force vs. central displacement for the specimens of configurations (a)-(c). configuration were tested. Two specimens of each The failure characteristics of all six test specimens are summarized in Figure 5. The recorded maximum loads and maximum central deflections of the beams at failure were quite close for three different configurations. In addition the failure characteristic of the six specimens is given I tabular form in Table 2. Specimen and configuration Failure load [N] a1 2307 a2 2332 b1 2094 b2 2106 c1 2185 c2 2246 Table 2 Failure characteristics of the tested specimens. Cross head Avg. cross head Avg. displacement displacement Location of failure load at failure at failure failure initiation [N] [mm] [mm] Compliant core 11.58 (51WF) 2320 11.78 Compliant core 11.97 (51WF) Compliant core 10.11 (51WF) 2100 9.96 Compliant core 9.80 (51WF) Compliant core 10.43 (51WF) 2216 10.83 Compliant core 11.22 (51WF) Completed delamination Yes Yes Yes Yes No No The average failure load measured for the specimens of configuration (c) was 2216N. This load level is within 5% of the average failure loads of configurations (a) and (b). Additionally, the central deflection at failure for configuration (c) is observed to be between the central deflections observed for configurations (a) and (b). This difference is estimated to be around 9%. In this connection it should be mentioned, that the short length of the weak core compared to the total length of the edge stiffeners and peel stoppers is the reason for the difference in central deflections observed for the improved (c) and conventional (a), (b) edge stiffeners. If the length of the pure core part of the sandwich structure was larger, compared to the total length of the embedded sub-structures, which would be the case for realistic design configurations, the difference in the ultimate displacements, and thus the influence of the peel stoppers on the overall structural stiffness of the sandwich, would be much smaller. Damage initiation and development of failure occurred according to the predicted scenario, as shown in Figures 6-8. High speed video recordings were used to identify the location of failure initiation and its progression in the sandwich specimens. In all cases, failure initiated as a shear crack in the centre of the weak core, the crack tip kinked towards the faces and continued as a delamination along face-core interfaces. Notice that a full delamination of the face occurs for the cases of conventional edge stiffeners (Figure 6and Figure 7), while the peel stopper in Figure 8 clearly confines the crack inside the weak core, and, moreover, lets the sandwich face still be attached to the sandwich beam edge. Figure 6 Failure of test specimen a1 Figure 7 Failure of test specimen b2 Figure 8 Failure of test specimen c2 The sandwich beams with embedded peel stoppers were subsequently loaded in the 3-point bending fixture in order to inspect the damage zone in the vicinity of the peel stoppers as seen in Figure 9. All beams of configurations (a) and (b) ended up with completely delaminated face sheets, while peel stoppers in configuration (c) effectively stopped delamination. Figure 9 Post mortem inspection of the cracked part of test specimen c2. Conclusions Three beam configurations were tested in a three point load condition and configuration (c) was equipped with the proposed peel stopper. Configuration (a) was considered due to its common practical design and configuration (b) and (c) had an Polyurethane insert embedded in its core. The only difference between configuration (b) and (c) was the particular shape of this embedded insert. The shape (internal curved boundary) of the polyurethane insert in configuration (c) was designed to arrest face-core peeling. Regarding the three considered configurations only configuration (c) was able to arrest face-core peeling and then confine the damage to an area in between the proposed peel stoppers. The presented concept may also be adapted to other types of structural sandwich elements (i.e. plates and shells) and then add security to future sandwich components. Acknowledgments The work presented was supported by the Danish Research Council for Technology and Production Sciences; Grant N 26-040160, “Structural Grading - a novel concept for design of sandwich sub-structures”, and the Innovation Consortium “Integrated Design and Processing of Lightweight Composite and Sandwich Structures” (abbreviated “KOMPOSAND”) funded by the Danish Ministry of Science, Technology and Development. The support received is gratefully acknowledged. The authors also acknowledge Degussa Röhm GmbH (Germany) for supplying the sandwich core materials used in this investigation. References 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. Jakobsen J., Bozhevolnaya E., Thomsen OT. "Peel Stopper for Sandwich Components". Patent Application: 2006-521/010184, December 8, 2006. Aalborg University, Denmark. Burman, M. & Zenkert, D., Int J Fatigue , vol 19(7), 551-561, 1997 Burman, M. & Zenkert, D., Int J Fatigue , vol 19(7), 563-578, 1997 Avilés, F. & Carlsson, L., J. Sandw. 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