CP620, Shock Compression of Condensed Matter - 2001 edited by M. D. Furnish, N. N. Thadhani, and Y. Horie © 2002 American Institute of Physics 0-7354-0068-7/02/$ 19.00 SPALL STRENGTH OF CERAMIC IN A MULTILAYER SYSTEM B.A.M. Vaughan, N.H. Murray7, W.G. Proud and J.E. Field PCS, Cavendish Laboratory, Madingley Road, Cambridge, CBS ONE. UK. } Now at Corus Group PLC. E-mail: nataliehmurray@hotmailcom Abstract. Investigations into the dynamic properties of alumina ceramic have been carried out for several years at the Cavendish Laboratory [1,2,3]- Previous work has demonstrated a reduction in spall strength with an increased width of the compression pulse using either thicker fliers, or a flier with longer double transit time for the shock wave. Here the variation in spall strength of an alumina ceramic as part of a multilayer system is investigated. Results indicate that the spall strength decreases with increasing time for which the target is under compression. There is some indication that spall strength may decrease faster under shock ring-up than a single shock taking the sample to the same ultimate pressure. interaction of rarefaction fans. These release fans are dispersive, which gives rise to a geometry dependence. INTRODUCTION Ceramics have been used in armour applications for several decades, first seeing use in the 1960's to protect American aircrews from small arms fire [4,5]. Their success is due to their inherent high compressive strength and low density, and are used whenever weight is a constraint [6]. Modern armour configurations are typically multi-layered structures consisting of ceramic and other materials such as metals and composites. Plate impact experiments have been performed on several types of alumina ceramic [2] to determine Hugoniots and other properties, including spall strength [1] and lateral stress. In the case of lateral stress, studies of ceramics with and without a cover plate of metal or ceramic between the flier and the target were performed [3]. The results show the importance of geometry on measured stress in the target, and prompted the current study, which is to investigate the spall strength of 880 alumina ceramic in several multilayer systems. The spall strength of a material can be determined experimentally by impact of plates of material, which are carried into tension through the ^reload C/5 Time FIGURE 1. Schematic representation of a gauge trace showing a target undergoing spall. The spall strength can be shown [7] to be given by ' spall 2ZU (1) where ZT and Zw refer to the impedance of the target material and to the PMMA window 747 independent measurement of the spall process. Three different target configurations were investigated and compared with previous studies [1]. The impact velocity in each case was selected to give rise to a ca. 4 GPa peak stress in the target. Table 1 shows the target configurations investigated. respectively, areload and amin are the stresses recorded by the gauge in the PMMA indicated in Fig. 1. For the target ceramic, the impedance is taken to be the elastic impedance, Z880 = p0cL, whereas for the PMMA window, the impedance at each stress state is determined from 7W = alIu p , using data taken from Marsh [8]. Figure 1 shows a schematic of a stress trace. The solution given in Eqn. (1) assumes elastic behaviour and is more appropriate in the case when TABLE 1. Target configuration Configuration Flier Cover (mm) plate (mm) 1 1.8 Cu 1.2 Al 2 1.8 Cu 1.2 Al 3 1.8 Cu 2.4 Al 4 3.0 Al None 5 3.0 880 None EXPERIMENTAL Experiments were carried out using the single stage 50-mm gas gun facility at the University of Cambridge [9]. Longitudinal stresses were measured by means of commercial manganin gauges (Micro Measurements type LM-SS-210FD050). These were placed in the 'back-surface' configuration as shown in Fig. 2. The calibration data of Rosenberg et al. [10] were used to convert the voltage data into stress. In addition, the pressure dependence of the impedance of the PMMA backing has been taken into account when calculating the stress in the target ceramic. It should be noted that if the impedance matched stress profile is used to measure oreioad and &min9 then Eqn. (1) reduces to Target thickness (mm) 4.0 11.0 4.0 12.0 6.0 RESULTS With the generic experimental arrangement shown in Fig. 2 the traces shown in Fig. 3 were obtained for the configurations 1-3. The back surface stress is converted to stress in 880 by an impedance matching technique that accounts for the change in impedance of PMMA with increasing stress. spall ~ °' load ~~ °" In some experiments, VISAR was used to record the PMMA-ceramic interface velocity, giving an Cu Al </> o 3. Gauge location 1 v•4—— Vpr 4—————— t PMMA Backing CD Q_ 0.2 -VISAR 1 880 Ceramic 59.75 FIGURE 2. Experimental arrangement for multiple step shock. The fliers were 1.8 mm OFHC copper, the target was 880 alumina ceramic and the buffer material was Dural (dimensions given in Table 1). The backing was 12 mm thick PMMA. 60.00 60.25 Time (us) FIGURE 3. Traces obtained for the calculated stress in 880 alumina ceramic. The corresponding VISAR traces are shown alongside. 748 wave speeds in the different targets. The time for which the sample is under compression until the release waves from the rear surfaces of the flier and target interact is denoted tspau. Table 2 contains the values of tspan for each of the arrangements and Fig. 5 shows a fit for this data. TABLE 2. Results Configuration tspall (US) 1 2 3 4 5 0.600 ± 0.2 0.604 ± 0.3 0.573± 0.2 0.942 ± 0.2 0.659 ± 0.2 Spall Strength (GPa) 0.214 ±0.08 0.127 ±0.156 0.535 ±0.07 0.356 ± 0.08 0.462 ± 0.09 It can be seen from Fig. 4 (configurations 1 and 2) that the thin aluminium buffer allows two compression pulses to reach the gauge plane before the release from the rear of the target arrives. Interactions deeper in the target and flier do not register on the gauge after the spall signal, and may be ignored. The situation at the gauge plane is similar to that of a single shock, as in [7] and cases 4,5. For the thick aluminium buffer (configuration 3), the spall signal reaches the PMMA-ceramic interface at approximately the same time as the second compression pulse, and may be thought of as a single shock of reduced strength. Those cases, 3-5, being single or approximately single shocks, have a higher spall strength than the two-step compression pulses with similar tspati It is unclear at this stage whether this is a physical consequence of the loading process, or the result of experimental scatter in the data. A two step loading pulse may weaken the material more effectively before the arrival of the release fan, which may explain these findings. 5) 880 CONCLUSION Spall strength in 880 alumina ceramic is dependent on the geometry of the system under investigation. We have found a correlation between the time the material is under compression until the release waves interact to form a spall plane, and the measured spall strength. This is consistent with previous work [1], which attributed the effect to the accumulation of damage in the form of microcracks. The longer the compressive stage be- x(mm) FIGURE 4. t-x diagrams for each of the configurations 1-5. The t-x diagrams corresponding to each of the configurations in Table 1 are shown schematically in Fig. 4. The release processes will manifest as release fans and will include waves both faster and slower than the initial shock wave. The lines shown are approximate, but show the relative positions of 749 1999, edited by Furnish, M.D., Chhabildas, L.C., and Hixson, R.S., American Institute of Physics, 2000 pp. 581-584. 4. Hannon, F. S. and Abbott, K. H., Materials Engineering, 68, (Sept. 1968) pp. 42-43 5. Rolston, R.F., Bodine, E., Dunleavy, J., Space/Astronautics, (July 1968), pp. 55-63 6. den Reijer, P.C., 4On the Penetration of Rods into Ceramic Faced Armours', Proc. 12th Int. Symp. Ballistics, 1, (1990) pp. 389-400 7. Grady, D.E. and Kipp, M.E., "Dynamic Fracture and Fragmentation" in High-Pressure Shock Compression of Solids /, edited by Asay, J.R. and Shahinpoor, M, Springer-Verlag, New York, 1993, pp. 265-322. 8. Marsh, S.P. "LASL Shock Hugoniot Data", University of California Press. 1980, pp. 446451 9. Bourne, N.K., Rosenberg, Z., Johnson, D.J., Field, J.E., Timbs, A.E. and Flaxman, R.P., Meas. Sci. Technol. 6, 1462-1470 (1995). 10. Rosenberg, Z., Yaviz, D. and Partom, Y. J. CO ±L Spall Strength, aspa|| (GPa) FIGURE 5. Measured spall strength using Eqn. (2), plotted against the time until release waves interact for each geometry. 1, 2 are 'double shock' results. fore spallation occurs, the more the microcracks can grow, generating larger flaws so that the tensile strength of the material is degraded. Additionally, there may be an effect due to the loading history, so that for a given compression time, tspau9 a single shock produced a higher spall strength than a steploading pulse caused by ringing up of stress in an intervening low impedance buffer. Detailed modelling of these situations using an appropriately sophisticated code and further experiments will be required to fully understand the data presented here. ACKNOWLEDGEMENTS The research was supported by DERA (Chertsey). We thank Drs I.M. Pickup and BJ. James for providing the materials and their continued interest in this work. D. L. A. Cross provided technical assistance. REFERENCES 1. 2. 3. Murray, N.H., Bourne, N.K., Rosenberg, Z. and Field, J.E., J. Appl. Phys. 84, No. 2, pp. 734738(1998). Murray, N.H., "The Response of Alumina Ceramics to Plate Impact Loading", PhD Thesis, University of Cambridge (1997). Murray, N.H., Millett, J.C.F., Proud, W.G. and Rosenberg, Z., "Issues Surrounding Lateral Stress Measurements in Alumina Ceramics", in Shock Compression of Condensed Matter 750
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